Week 1 - 8/28
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Week 2
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9/4 Reductive Amination: experimental procedure blank reagent table |
Week 3 - 9/11 Grignard Procedure |
Week 4 - 9/18 |
Week 5 - 9/25 |
Week 6 - 10/2 Explore "Extract Twice with Ether" Part A Report instructions & |
Week 7 - 10/9 |
Week 8
- 10/16
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Week 9 - 10/23
Introduction to Mass Spectrometry |
Week 10 - 10/30 |
Week 11 - 11/6 |
Week 12
- 11/13 Acylation of Ferrocene Procedure Include a sketch in your notebook! Due next week @ start of lab TLC simulator worksheet Canvas: TLC quiz |
Week 13 - 11/20 |
Week 14 - 11/27 |
Week 15
- 12/4 |
Sample notebook pages
Reagent Table practice: blank table | answer key | video solution
Spectroscopy handouts (IR, NMR, Mass Spec)
1H NMR introduction lecture (1.5 hours)
sample NMR problem answer key
Lab techniques: tutorials (Distillation, Extraction, TLC, Recrystallization, Melting Point)
O-Chem Lab Techniques eBook: FREE downloadable pdf with lots of great pictures Lab Manual (PDF) (Table of Contents) Online Lab Manual
Got Workups? What does it mean to work-up a reaction? What are some typical steps? Check out Chem LibreText for a discussion and overview.
MIT OpenCourseWare: Lab Videos and Digital Lab Techniques Manual
Kimberly Berkowski, Sarah Tabacco, Aayesha Siddiqui, and Eileen Huang. RES.5-0001 Digital Lab Techniques Manual. Spring 2007. Massachusetts Institute of Technology: MIT OpenCourseWare, https://ocw.mit.edu. License: Creative Commons."Not Voodoo" website - collection of practical techniques, tips and tricks
TLC simulator (video)
TLC (Thin-Layer Chromatography)
- interactive TLC simulation (and worksheet)
- simulation walk-through video
- Information and recipes for TLC stains
Extraction
interactive animation (and worksheet)
animation walk-through video
Extraction animation (video)
Column Chromatography:
- Wikipedia entry
- W. Clark Still JOC article on rapid "flash" columns (reading guide)
- MIT video
- Not Voodoo website
Fractional Distillation apparatus: interactive picture and handout
Free chemical drawing software! Did you know that your institution has purchased a Site Subscription through PerkinElmer Informatics, makers of ChemBioDraw Ultra 13.0? This means that you are able to download fully functional chemistry or biology software and have access to online databases, via the Cal Poly Pomona site subscription, which has been prepaid by your institution.You are able to download as long as you have a valid cpp.edu email. Click here to download ChemBioDraw Ultra 13.0, and access any related database subscriptions.
Mass Spec calculator ChemCalc (determines possible formulas, given a molecular or fragment mass)
"ChemCalc: a building block for tomorrow’s chemical infrastructure." Patiny, Luc; Borel, Alain
Journal of Chemical Information and Modeling 201. DOI: http://dx.doi.org/10.1021/ci300563h
Dr. Starkey's Web Page |
Cal Poly Pomona Web Page |
Chemistry Department Web Page |
Last updated November 11, 2024